Reaction & separation
Mechanical Operations
5 self-contained study topics — notes, diagrams, formulas, and worked examples for exams and GATE.
Topics
- Particle Size ReductionSize-reduction energy is estimated from comminution laws — Kick’s for coarse crushing, Rittinger’s for fine grinding, and Bond’s (via the work index) for the intermediate range that covers most industrial mills.
- Screening and ClassificationScreening separates particles by size against an aperture, and classification separates by settling velocity in a fluid; performance is judged by screen efficiency and by the cut size d₅₀ at which a particle has equal chance of reporting to either stream.
- FiltrationCake filtration is modelled by adding the growing cake resistance to a constant medium resistance; at constant pressure the filtrate volume follows a parabolic law, and plotting t/V against V linearises the data to extract specific cake resistance α and medium resistance R_m.
- Sedimentation and CentrifugationGravity settling is governed by Stokes’ terminal velocity (valid only for particle Reynolds number below one), and a centrifuge simply replaces g with the far larger centrifugal acceleration rω², dramatically speeding separation of fine particles.
- FluidizationFluidization occurs when upward gas velocity is high enough that the bed pressure drop equals the bed weight per unit area; beyond the minimum fluidization velocity the pressure drop stays constant while the bed expands and behaves like a boiling liquid.